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Beilstein J. Org. Chem. 2009, 5, No. 62, doi:10.3762/bjoc.5.62
Graphical Abstract
Scheme 1: Mesogenic imidazolium synthesis [Reaction conditions: (i) DMF, K2CO3, BrCnH2n+1, 60 °C, overnight; ...
Scheme 2: Anion exchange in water.
Figure 1: 1H NMR spectrum (in CD2Cl2) of 110–610.
Figure 2: TGA measurements of wet and water free 112 imidazolium salt.
Figure 3: TGA measurements of the two entire series 110–610 and 114–614 (rate 10° C·min−1, in air).
Figure 4: Transition temperatures of 114–614 as a function of the anion (Cr = crystal; SmA: smectic A phase; ...
Figure 5: (a) Illustration of a single homeotropic monodomain, which is observed as a black isotropic texture...
Figure 6: Diffraction small-angle X-ray pattern of the smectic phase of 212 recorded at T = 100 °C.
Figure 7: Variation with the counter-ion of the molecular area S and of the ionic sublayer thickness dc (incl...
Figure 8: Grazing incidence X-ray pattern at 100 °C on the top of a 312 droplet, slowly cooled down from isot...
Figure 9: Variations with chain length of the maximum molecular areas close to isotropization Smax and of the...